185815-59-2, 4-Isobutyldihydro-2H-pyran-2,6(3H)-dione is a Tetrahydropyrans compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
Example 3: Preparation of 3-aminomethyl-N,N-diethyI-5-methylhexanamide.; Step a): Preparation of 3-(2-(diethyl amino)-2-oxoethyl)-methylhexanoic acid; To a solution of 3- isobutyl glutaric anhydride (5 grams) in dichloromethane(10 ml), added diethyl amine (4.3 grams) and stirred the reaction mixture for 12 hrs at 250C. The reaction mixture was quenched with water (10 ml) and the pH of the reaction mixture adjusted to 1.0 using hydrochloric acid. The organic layer was separated and the aqueous layer was extracted with dichloromethane. The organic layers were combined and the solvent distilled off to provide the title compound as a residue. Yield: 6.5 grams, 185815-59-2
The synthetic route of 185815-59-2 has been constantly updated, and we look forward to future research findings.
Reference£º
Patent; SATYANARAYANA REDDY, Manne; THIRUMALAI RAJAN, Srinivasan; ESWARAIAH, Sajja; SATYANARAYANA, Revu; WO2009/1372; (2008); A2;,
Tetrahydropyran – Wikipedia
Tetrahydropyran – an overview | ScienceDirect Topics