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Treatments of fully acetylated sugars with bis(tributyltin) oxide in toluene at reflux, and with potassium cyanide or potassium hydroxide, or both, in mixtures of tetrahydrofuran and 2-propanol were found to be effective for regioselective 1-O-deacetylation of fully acetylated sugars.
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Reference：
Tetrahydropyran – Wikipedia,
Tetrahydropyran – an overview | ScienceDirect Topics