1152567-60-6, 4-(4-Bromophenyl)tetrahydro-2H-pyran-4-carboxylic acid is a Tetrahydropyrans compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
Method 52 Synthesis of 2-[4-(4-bromophenyl)tetrahydropyran-4-yl]-1H-benzimidazole (Intermediate 77) A mixture of I-51.2 (50 mg, 0.175 mmol), phenylenediamine (23 mg, 0.210 mmol), and triphenylphosphite (60 muL, 0.228 mmol) in pyridine (1 mL) is sealed in a vessel and heated at 150 C. for 18 h. After cooling to room temperature the reaction is diluted with DCM and washed with saturated aqueous NaHCO3. The organics are dried over anhydrous Na2SO4 and concentrated in vacuo. Purification is by flash chromatography (SiO2, DCM to 3% MeOH in DCM) to give the title intermediate I-79 (46 mg) m/z 357.0, 358.8 [M+H]., 1152567-60-6
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Reference£º
Patent; BARTOLOZZI, Alessandra; CHEN, Zhidong; DINES, Jonathon Alan; LO, Ho Yin; LOKE, Pui Leng; OLAGUE, Alan; RIETHER, Doris; TYE, Heather; WU, Lifen; ZINDELL, Renee M.; US2013/196967; (2013); A1;,
Tetrahydropyran – Wikipedia
Tetrahydropyran – an overview | ScienceDirect Topics